Confocal micro-XRF spectroscopy using synchrotron or conventional X-ray source based excitation
is becoming a well-established microanalytical method providing three-dimensional (3D)
information on the elemental distributions in the probed sample volume with trace-level detection
limits. Additionally, full-field micro XAS spectroscopy has recently been shown to allow for 3D
structural analysis in previously infeasible time frames. This proposal aims the further
development of quantitative 3D confocal XRF and XAS techniques for the detailed non-destructive
and contamination free study of rare-earth element compositional information of unique
extraterrestrial materials. The project will focus on photon trajectory simulation through X-ray
optics as a novel extension to currently available Monte Carlo based XRF quantification routines,
as well as further developing 3D structural analysis by means of state-of-the-art full-field XAS
methodologies. The experimental studies will be performed in close collaboration with the
NanoGeoscience group lead by Prof. F.E. Brenker (Johann Wolfgang Goethe-University, Frankfurt,
Germany) in the framework of approved research projects at the P06 Hard X-ray
Micro/Nanoprobe at the new PETRA III synchrotron radiation facility (Hamburg, Germany) and
DUBBLE beamline (BM26 and BM14) at the ESRF (Grenoble, France) synchrotron radiation
facilities.