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Researcher
Frank Bosmans
Profile
Projects
Publications
Activities
Awards & Distinctions
78
Results
2024
Anxiety and dysautonomia symptoms in patients with a NaV1.7 mutation and the potential benefits of low-dose short-acting guanfacine
Rita de Cassia de Oliveira Collaco
Maxime Lammens
Carley Blevins
Kristen Rodgers
Andrei Gurau
Suguru Yamauchi
Christine Kim
Jeannine Forrester
Edward Liu
Jinny Ha
et al.
A1
Journal Article
in
CLINICAL AUTONOMIC RESEARCH
2024
Exploring cardiac sympathetic denervation as a treatment approach for recurrent ventricular arrhythmias : a concise review
Andrei Gurau
Frank Bosmans
Andreas Barth
Malcolm V Brock
Jinny S Ha
A2
Journal Article
in
JOURNAL OF CLINICAL & EXPERIMENTAL CARDIOLOGY
2024
2023
Structure-function relationship of new peptides activating human Nav1.1
Ludivine Lopez
Stephan De Waard
Hervé Meudal
Cécile Caumes
Kuldip Khakh
Steve Peigneur
Barbara Oliveira-Mendes
Sophia Lin
Jolien De Waele
Jérôme Montnach
et al.
A1
Journal Article
in
BIOMEDICINE & PHARMACOTHERAPY
2023
Understanding the physiological role of NaV1.9 : challenges and opportunities for pain modulation
Wayra Brackx
Rita de Cassia de Oliveira Collaco
Margaux Theys
Jolien Vander Cruyssen
Frank Bosmans
A1
Journal Article
in
PHARMACOLOGY & THERAPEUTICS
2023
2022
In vivo spatiotemporal control of voltage-gated ion channels by using photoactivatable peptidic toxins
Jérôme Montnach
Laila Ananda Blömer
Ludivine Lopez
Luiza Filipis
Hervé Meudal
Aude Lafoux
Sébastien Nicolas
Duong Chu
Cécile Caumes
Rémy Béroud
et al.
A1
Journal Article
in
NATURE COMMUNICATIONS
2022
N-type inactivation variances in honeybee and Asian giant hornet Kv channels
Shahid Hussain
Jolien De Waele
Maxime Lammens
Frank Bosmans
A2
Journal Article
in
BIOELECTRICITY
2022
Neonatal Nav1.5 : pharmacological distinctiveness of a cancer‐related voltage‐gated sodium channel splice variant
Scott P. Fraser
Rustem Onkal
Margaux Theys
Frank Bosmans
Mustafa B. A. Djamgoz
A1
Journal Article
in
BRITISH JOURNAL OF PHARMACOLOGY
2022
2021
Getting stoned : characterisation of the coagulotoxic and neurotoxic effects of reef stonefish (Synanceia verrucosa) venom
Richard J. Harris
Nicholas J. Youngman
Weili Chan
Frank Bosmans
Karen L. Cheney
Bryan G. Fry
A1
Journal Article
in
TOXICOLOGY LETTERS
2021
Homozygous SCN1B variants causing early infantile epileptic encephalopathy 52 affect voltage-gated sodium channel function
Marcello Scala
Stephanie Efthymiou
Tipu Sultan
Jolien De Waele
Marta Panciroli
Vincenzo Salpietro
Reza Maroofian
Pasquale Striano
Filip Van Petegem
Henry Houlden
et al.
A1
Journal Article
in
EPILEPSIA
2021
The dragon’s paralysing spell : evidence of sodium and calcium ion channel binding neurotoxins in Helodermatid and Varanid lizard venoms
James S. Dobson
Richard J. Harris
Christina N. Zdenek
Tam Huynh
Wayne C. Hodgson
Frank Bosmans
Rudy Fourmy
Aude Violette
Bryan G. Fry
A1
Journal Article
in
TOXINS
2021
2020
Australian funnel-web spiders evolved human-lethal δ-hexatoxins for defense against vertebrate predators
V Herzig
K Sunagar
DTR Wilson
SS Pineda
MR Israel
S Dutertre
BS McFarland
EAB Undheim
WC Hodgson
PF Alewood
et al.
A1
Journal Article
in
PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA
2020
Biophysical investigation of sodium channel interaction with β-subunit variants associated with arrhythmias
José P. Llongueras
Samir Das
Jolien De Waele
Lucio Capulzini
Antonio Sorgente
Filip Van Petegem
Frank Bosmans
A2
Journal Article
in
BIOELECTRICITY
2020
Mutational analysis of ProTx-I and the novel venom peptide Pe1b provide insight into residues responsible for selective inhibition of the analgesic drug target NaV1.7
Darshani B. Rupasinghe
Volker Herzig
Irina Vetter
Zoltan Dekan
John Gilchrist
Frank Bosmans
Paul F. Alewood
Richard J. Lewis
Glenn F. King
A1
Journal Article
in
BIOCHEMICAL PHARMACOLOGY
2020
2019
Chemical synthesis, proper folding, Nav channel selectivity profile and analgesic properties of the spider peptide phlotoxin 1
S Nicolas
C Zoukimian
Frank Bosmans
J Montnach
S Diochot
E Cuypers
S De Waard
R Béroud
D Mebs
D Craik
et al.
A1
Journal Article
in
TOXINS
2019
Structural basis of α-scorpion toxin action on Nav channels
Thomas Clairfeuille
Alexander Cloake
Daniel T Infield
José P Llongueras
Christopher P Arthur
Zhong Rong Li
Yuwen Jian
Marie-France Martin-Eauclaire
Pierre E Bougis
Claudio Ciferri
et al.
A1
Journal Article
in
SCIENCE
2019
2018
A disease mutation reveals a role for Nav1.9 in acute itch
Juan Salvatierra
Marcelo Diaz-Bustamante
James Meixiong
Elaine Tierney
Xinzhong Dong
Frank Bosmans
A1
Journal Article
in
JOURNAL OF CLINICAL INVESTIGATION
2018
Nav1.1 inhibition can reduce visceral hypersensitivity
Juan Salvatierra
Joel Castro
Andelain Erickson
Qian Li
João Braz
John Gilchrist
Luke Grundy
Grigori Y Rychkov
Annemie Deiteren
Rana Rais
et al.
A1
Journal Article
in
JCI INSIGHT
2018
Spider toxin inhibits gating pore currents underlying periodic paralysis
Roope Männikkö
Zakhar O Shenkarev
Michael G Thor
Antonina A Berkut
Mikhail Yu Myshkin
Alexander S Paramonov
Dmitrii S Kulbatskii
Dmitry A Kuzmin
Marisol Sampedro Castañeda
Louise King
et al.
A1
Journal Article
in
PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA
2018
Using voltage-sensor toxins and their molecular targets to investigate Nav1.8 gating
John Gilchrist
Frank Bosmans
A1
Journal Article
in
JOURNAL OF PHYSIOLOGY-LONDON
2018
2017
Insect-active toxins with promiscuous pharmacology from the African theraphosid spider Monocentropus balfouri
Jennifer J Smith
Volker Herzig
Maria P Ikonomopoulou
Slawomir Dziemborowicz
Frank Bosmans
Graham M Nicholson
Glenn F King
A1
Journal Article
in
TOXINS
2017
Pharmacological characterisation of the highly Nav1.7 selective spider venom peptide Pn3a
Jennifer R Deuis
Zoltan Dekan
Joshua S Wingerd
Jennifer J Smith
Nehan R Munasinghe
Rebecca F Bhola
Wendy L Imlach
Volker Herzig
David A Armstrong
K Johan Rosengren
et al.
A1
Journal Article
in
SCIENTIFIC REPORTS
2017
Pharmacology of the Nav1.1 domain IV voltage sensor reveals coupling between inactivation gating processes
Jerremiah D Osteen
Kevin Sampson
Vivek Iyer
David Julius
Frank Bosmans
A1
Journal Article
in
PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA
2017
Sodium channel Nav1.8 underlies TTX-resistant axonal action potential conduction in somatosensory C-fibers of distal cutaneous nerves
Amanda H Klein
Alina Vyshnevska
Timothy V Hartke
Roberto De Col
Joseph L Mankowski
Brian Turnquist
Frank Bosmans
Peter W Reeh
Martin Schmelz
Richard W Carr
et al.
A1
Journal Article
in
JOURNAL OF NEUROSCIENCE
2017
The tarantula toxin β/δ-TRTX-Pre1a highlights the importance of the S1-S2 voltage-sensor region for sodium channel subtype selectivity
Joshua S Wingerd
Christine A Mozar
Christine A Ussing
Swetha S Murali
Yanni K-K Chin
Ben Cristofori-Armstrong
Thomas Durek
John Gilchrist
Christopher W Vaughan
Frank Bosmans
et al.
A1
Journal Article
in
SCIENTIFIC REPORTS
2017
2016
A painful tale about synthetic scorpion toxins
Juan Salvatierra
Frank Bosmans
Editorial material
2016
Binary architecture of the Nav1.2-β2 signaling complex
Samir Das
John Gilchrist
Frank Bosmans
Filip Van Petegem
A1
Journal Article
in
ELIFE
2016
Efficient enzymatic cyclization of an inhibitory cystine knot-containing peptide
Soohyun Kwon
Frank Bosmans
Quentin Kaas
Olivier Cheneval
Anne C Conibear
K Johan Rosengren
Conan K Wang
Christina I Schroeder
David J Craik
A1
Journal Article
in
BIOTECHNOLOGY AND BIOENGINEERING
2016
Isolation of two insecticidal toxins from venom of the Australian theraphosid spider Coremiocnemis tropix
Maria P Ikonomopoulou
Jennifer J Smith
Volker Herzig
Sandy S Pineda
Slawomir Dziemborowicz
Sing-Yan Er
Thomas Durek
John Gilchrist
Paul F Alewood
Graham M Nicholson
et al.
A1
Journal Article
in
TOXICON
2016
Molecular basis of the remarkable species selectivity of an insecticidal sodium channel toxin from the African spider Augacephalus ezendami
Volker Herzig
Maria Ikonomopoulou
Jennifer J Smith
Slawomir Dziemborowicz
John Gilchrist
Lucia Kuhn-Nentwig
Fernanda Oliveira Rezende
Luciano Andrade Moreira
Graham M Nicholson
Frank Bosmans
et al.
A1
Journal Article
in
SCIENTIFIC REPORTS
2016
Selective spider toxins reveal a role for the Nav1.1 channel in mechanical pain
Jeremiah D Osteen
Volker Herzig
John Gilchrist
Joshua J Emrick
Chuchu Zhang
Xidao Wang
Joel Castro
Sonia Garcia-Caraballo
Luke Grundy
Grigori Y Rychkov
et al.
A1
Journal Article
in
NATURE
2016
The hitchhiker's guide to the voltage-gated sodium channel galaxy
Christopher A Ahern
Jian Payandeh
Frank Bosmans
Baron Chanda
A1
Journal Article
in
JOURNAL OF GENERAL PHYSIOLOGY
2016
The scorpion toxin Bot IX is a potent member of the α-like family and has a unique N-terminal sequence extension
Marie-France Martin-Eauclaire
Juan Salvatierra
Pascal Mansuelle
Frank Bosmans
Pierre E Bougis
A1
Journal Article
in
FEBS LETTERS
2016
2015
A surface plasmon resonance approach to monitor toxin interactions with an isolated voltage-gated sodium channel paddle motif
Marie-France Martin-Eauclaire
Geraldine Ferracci
Frank Bosmans
Pierre E Bougis
A1
Journal Article
in
JOURNAL OF GENERAL PHYSIOLOGY
2015
From foe to friend: using animal toxins to investigate ion channel function.
Jeet Kalia
Mirela Milescu
Juan Salvatierra
Jordan Wagner
Julie K Klint
Glenn F King
Baldomero M Olivera
Frank Bosmans
A1
Journal Article
in
JOURNAL OF MOLECULAR BIOLOGY
2015
MmTX1 and MmTX2 from coral snake venom potently modulate GABAa receptor activity
Jean-Pierre Rosso
Jürgen R Schwarz
Marcelo Diaz-Bustamante
Brigitte Céard
José M Gutiérrez
Matthias Kneussel
Olaf Pongs
Frank Bosmans
Pierre E Bougis
A1
Journal Article
in
PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA
2015
Seven novel modulators of the analgesic target Nav1.7 uncovered using a high-throughput venom-based discovery approach
Julie K Klint
Jennifer J Smith
Irina Vetter
Darshani B Rupasinghe
Sing Yan Er
Sebastian Senff
Volker Herzig
Mehdi Mobli
Richard J Lewis
Frank Bosmans
et al.
A1
Journal Article
in
Br J Pharmacol
2015
The insecticidal spider toxin SFI1 is a knottin peptide that blocks the pore of insect voltage-gated sodium channels via a large β-hairpin loop
Niraj S Bende
Slawomir Dziemborowicz
Volker Herzig
Venkatraman Ramanujam
Geoffrey W Brown
Frank Bosmans
Graham M Nicholson
Glenn F King
Mehdi Mobli
A1
Journal Article
in
FEBS JOURNAL
2015
The scorpion toxin Tf2 from Tityus fasciolatus promotes Nav1.3 opening
Thalita S Camargos
Frank Bosmans
Solange C Rego
Caroline BF Mourão
Elisabeth F Schwartz
A1
Journal Article
in
PLOS ONE
2015
2014
A distinct sodium channel voltage-sensor locus determines insect selectivity of the spider toxin Dc1a
Niraj S Bende
Slawomir Dziemborowicz
Mehdi Mobli
Volker Herzig
John Gilchrist
Jordan Wagner
Graham M Nicholson
Glenn F King
Frank Bosmans
A1
Journal Article
in
NATURE COMMUNICATIONS
2014
A first exploration of the venom of the Buthus occitanus scorpion found in southern France
Marie-France Martin-Eauclaire
Frank Bosmans
Brigitte Céard
Sylvie Diochot
Pierre E Bougis
A1
Journal Article
in
TOXICON
2014
Animal toxins influence voltage-gated sodium channel function
John Gilchrist
Baldomero M Olivera
Frank Bosmans
Bookchapter
in
Voltage gated sodium channels
2014
Nav1.1 modulation by a novel triazole compound attenuates epileptic seizures in rodents
John Gilchrist
Stacey Dutton
Marcelo Diaz-Bustamante
Annie McPherson
Nicolas Olivares
Jeet Kalia
Andrew Escayg
Frank Bosmans
A1
Journal Article
in
ACS CHEMICAL BIOLOGY
2014
2013
Crystallographic insights into sodium-channel modulation by the β4 subunit
John Gilchrist
Samir Das
Filip Van Petegem
Frank Bosmans
A1
Journal Article
in
PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA
2013
New rule(r)s for FRET
Frank Bosmans
Other
2013
The insecticidal neurotoxin Aps III is an atypical knottin peptide that potently blocks insect voltage-gated sodium channels
Niraj S Bende
Eunji Kang
Volker Herzig
Frank Bosmans
Graham M Nicholson
Mehdi Mobli
Glenn F King
A1
Journal Article
in
BIOCHEMICAL PHARMACOLOGY
2013
2012
Animal toxins can alter the function of Nav1.8 and Nav1.9
John Gilchrist
Frank Bosmans
A1
Journal Article
in
TOXINS
2012
2011
Functional properties and toxin pharmacology of a dorsal root ganglion sodium channel viewed through its voltage sensors
Frank Bosmans
Michelino Puopolo
Marie-France Martin-Eauclaire
Bruce P Bean
Kenton J Swartz
A1
Journal Article
in
JOURNAL OF GENERAL PHYSIOLOGY
2011
Palmitoylation influences the function and pharmacology of sodium channels
Frank Bosmans
Mirela Milescu
Kenton J Swartz
A1
Journal Article
in
PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA
2011
2010
Targeting voltage sensors in sodium channels with spider toxins
Frank Bosmans
Kenton J Swartz
A1
Journal Article
in
TRENDS IN PHARMACOLOGICAL SCIENCES
2010
2009
Insecticidal peptides from the theraposid spider Brachypelma albiceps : an NMR-based model of Ba2
Gerardo Corzo
Cedric Bernard
Herlinda Clement
Elba Villegas
Frank Bosmans
Jan Tytgat
Lourival D Possani
Hervé Darbon
Alejandro Alagón
A1
Journal Article
in
BIOCHIMICA ET BIOPHYSICA ACTA-PROTEINS AND PROTEOMICS
2009
Interactions between lipids and voltage sensor paddles detected with tarantula toxins
Mirela Milescu
Frank Bosmans
Seungkyu Lee
AbdulRasheed A Alabi
Jae Il Kim
Kenton J Swartz
A1
Journal Article
in
NATURE STRUCTURAL & MOLECULAR BIOLOGY
2009
2008
Animal peptides targeting voltage-activated sodium channels.
Bert Billen
Frank Bosmans
Jan Tytgat
A1
Journal Article
in
CURRENT PHARMACEUTICAL DESIGN
2008
Biochemical characterization of cysteine-rich peptides from Oxyopes sp. venom that block calcium ion channels
Elba Villegas
Satomi Adachi-Akahane
Frank Bosmans
Jan Tytgat
Terumi Nakajima
Gerardo Corzo
A1
Journal Article
in
TOXICON
2008
Deconstructing voltage sensor function and pharmacology in sodium channels
Frank Bosmans
Marie-France Martin-Eauclaire
Kenton J Swartz
A1
Journal Article
in
NATURE
2008
2007
Differential effects of five 'classical' scorpion beta-toxins on rNav1.2a and DmNav1 provide clues on species-selectivity
Frank Bosmans
Marie-France Martin-Eauclaire
Jan Tytgat
A1
Journal Article
in
TOXICOLOGY AND APPLIED PHARMACOLOGY
2007
Sea anemone venom as a source of insecticidal peptides acting on voltage-gated Na+ channels
Frank Bosmans
Jan Tytgat
A1
Journal Article
in
TOXICON
2007
Solution structure and alanine scan of a spider toxin that affects the activation of mammalian voltage-gated sodium channels
Gerardo Corzo
Jennifer K Sabo
Frank Bosmans
Bert Billen
Elba Villegas
Jan Tytgat
Raymond S Norton
A1
Journal Article
in
JOURNAL OF BIOLOGICAL CHEMISTRY
2007
Spider peptide toxins as leads for drug development
Pierre Escoubas
Frank Bosmans
A1
Journal Article
in
EXPERT OPINION ON DRUG DISCOVERY
2007
Voltage-gated sodium channel modulation by scorpion α-toxins
Frank Bosmans
Jan Tytgat
A1
Journal Article
in
TOXICON
2007
2006
Four novel tarantula toxins as selective modulators of voltage-gated sodium channel subtypes
Frank Bosmans
L Rash
S Zhu
S Diochot
M Lazdunski
P Escoubas
J Tytgat
A1
Journal Article
in
MOLECULAR PHARMACOLOGY
2006
The first potassium channel toxin from the venom of the Iranian scorpion Odonthobuthus doriae
Yousra Abdel-Mottaleb
Elke Clynen
Amir Jalali
Frank Bosmans
Hossein Vatanpour
Liliane Schoofs
Jan Tytgat
A1
Journal Article
in
FEBS LETTERS
2006
2005
BjαIT : a novel scorpion α-toxin selective for insects : unique pharmacological tool
Tal Arnon
Tamara Potikha
Daniel Sher
Menashe Elazar
Wenfu Mao
Tzachy Tal
Frank Bosmans
Jan Tytgat
Nissim Ben-Arie
Eliahu Zlotkin
A1
Journal Article
in
INSECT BIOCHEMISTRY AND MOLECULAR BIOLOGY
2005
Expression, renaturation and functional analysis of an excitatory insect-specific toxin from scorpion Buthus martensii Karsch
C Li
W Liu
Frank Bosmans
RH Zhu
J Tytgat
DC Wang
A1
Journal Article
in
PROTEIN AND PEPTIDE LETTERS
2005
Molecular basis of the mammalian potency of the scorpion α-like toxin, BmK M1
LH Liu
Frank Bosmans
C Maertens
RH Zhu
DC Wang
J Tytgat
A1
Journal Article
in
FASEB JOURNAL
2005
New 'Birtoxin analogs' from Androctonus australis venom
MF Martin-Eauclaire
B Ceard
Frank Bosmans
JP Rosso
J Tytgat
PE Bougis
A1
Journal Article
in
BIOCHEMICAL AND BIOPHYSICAL RESEARCH COMMUNICATIONS
2005
OD1, the first toxin isolated from the venom of the scorpion Odonthobuthus doriae active on voltage-gated Na+ channels
A Jalali
Frank Bosmans
M Amininasab
E Clynen
E Cuypers
A Zaremirakabadi
MN Sarbolouki
L Schoofs
H Vatanpour
J Tytgat
A1
Journal Article
in
FEBS LETTERS
2005
Pharmacological comparison of two different insect models using the scorpion α-like toxin BmK M1 from Buthus martensii Karsch
Frank Bosmans
B Brône
YM Sun
RH Zhu
YM Xiong
DC Wang
E Van Kerkhove
J Tytgat
A1
Journal Article
in
PROTEIN AND PEPTIDE LETTERS
2005
Solution structure of two insect-specific spider toxins and their pharmacological interaction with the insect voltage-gated Na+ channel
G Ferrat
Frank Bosmans
J Tytgat
C Pimentel
B Chagot
N Gilles
T Nakajima
H Darbon
G Corzo
A1
Journal Article
in
PROTEINS-STRUCTURE FUNCTION AND BIOINFORMATICS
2005
Structural basis for the voltage-gated Na+ channel selectivity of the scorpion α-like toxin BmK M1
X Ye
Frank Bosmans
C Li
Y Zhang
DC Wang
J Tytgat
A1
Journal Article
in
JOURNAL OF MOLECULAR BIOLOGY
2005
The depressant scorpion neurotoxin LqqIT2 selectively modulates the insect voltage-gated sodium channel
Frank Bosmans
Marie-France Martin-Eauclaire
Jan Tytgat
A1
Journal Article
in
TOXICON
2005
2004
Adaptive evolution of scorpion sodium channel toxins.
SY Zhu
Frank Bosmans
J Tytgat
A1
Journal Article
in
JOURNAL OF MOLECULAR EVOLUTION
2004
Phaiodotoxin, a novel structural class of insect-toxin isolated from the venom of the Mexican scorpion Anuroctonus phaiodactylus
Norma A Valdez-Cruz
Cesar VF Batista
Fernando Z Zamudio
Frank Bosmans
Jan Tytgat
Lourival D Possani
A1
Journal Article
in
EUROPEAN JOURNAL OF BIOCHEMISTRY
2004
The poison Dart frog's batrachotoxin modulates Nav1.8
Frank Bosmans
C Maertens
F Verdonck
J Tytgat
A1
Journal Article
in
FEBS LETTERS
2004
2003
Characterization of Amm VIII from Androctonus mauretanicus mauretanicus : a new scorpion toxin that discriminates between neuronal and skeletal sodium channels
M Alami
H Vacher
Frank Bosmans
C Devaux
JP Rosso
PE Bougis
J Tytgat
H Darbon
MF Martin-Eauclaire
A1
Journal Article
in
BIOCHEMICAL JOURNAL
2003
Function and solution structure of hainantoxin-I, a novel insect sodium channel inhibitor from the Chinese bird spider Selenocosmia hainana
Dongling Li
Yucheng Xiao
Weijun Hu
Jinyun Xie
Frank Bosmans
Jan Tytgat
Songping Liang
A1
Journal Article
in
FEBS LETTERS
2003
Importance of the conserved aromatic residues in the scorpion α-like toxin BmK M1 : the hydrophobic surface region revisited
YM Sun
Frank Bosmans
RH Zhu
C Goudet
YM Xiong
J Tytgat
DC Wang
A1
Journal Article
in
JOURNAL OF BIOLOGICAL CHEMISTRY
2003
2002
The sea anemone Bunodosoma granulifera contains surprisingly efficacious and potent insect-selective toxins
Frank Bosmans
A Aneiros
J Tytgat
A1
Journal Article
in
FEBS LETTERS
2002
1998
Liquid chromatographic method for separation of lincomycin from its related substances
Jennifer Orwa
Frank Bosmans
S Depuydt
E Roets
Jos Hoogmartens
A1
Journal Article
in
JOURNAL OF CHROMATOGRAPHY A
1998